特点:
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通过更严格的UHPLC测试,极低的背景基线和杂质干扰(如邻苯二甲酸酯和聚乙二醇等)
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通过UHPLC-MS TOF正离子和负离子模式测试,在模式切换时不会产生剧烈的基线漂移
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包装于白色硅硼酸盐玻璃瓶中,有效避免碱金属加合物的生成
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经0.1 μm膜过滤,不增加溶剂产生的背压
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极高的批次重现性
grade LC-MS Ultra CHROMASOLV®
vapor density 1.11 (vs air)
vapor pressure 410 mmHg ( 50 °C)
97.68 mmHg ( 20 °C)
assay ≥99.9% (GC)
autoignition temp. 725 °F
quality tested for UHPLC-MS
shelf life (limited shelf life, expiry date on the label)
expl. lim. 36 %
total impurities ≤0.0001% free alkali (as NH3)
≤0.0001% non-volatile
≤0.002% free acid (as CH3COOH)
≤0.03% water
≤0.3 ppb fluorescence (as quinine) at 365 nm
≤0.5 ppb fluorescence (as quinine) at 254 nm
transmittance 210 nm, ≥40%
220 nm, ≥65%
230 nm, ≥80%
260 nm, ≥98%
refractive index n20/D 1.329(lit.)
bp 64.7 °C(lit.)
mp −98 °C(lit.)
density 0.791 g/mL at 25 °C(lit.)
cation traces Al: ≤0.02 mg/kg
Ca: ≤0.05 mg/kg
Fe: ≤0.02 mg/kg
K: ≤0.05 mg/kg
Mg: ≤0.02 mg/kg
Na: ≤0.1 mg/kg
abs. UHPLC-gradient/220 nm ≤15 mAU (drift)
UHPLC-gradient/220 nm ≤8 mAU (peak)
UHPLC-gradient/235 nm ≤4 mAU (peak)
UHPLC-gradient/235 nm ≤8 mAU (drift)
suitability passes test for suitability for UHPLC-MS